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The principle of operation of the AFM is shown on the left picture.
A cantilever with very sharp tip (radius < 1 nm) at one end is oscillated at
its resonance frequency in close proximity to the surface of interest. The tip is
scanned in X-Y plane. The tip-surface interaction is measured. This interaction
can be due to Van der Waals forces and then a 3D topography is displayed in AFM.
Or the forces can be due to electrical, mechanical, optical, frictional, interactions
and these properties of the surface can be mapped with 50 nm down to single atom
resolutions. There are more then 20 methods that measure different interactions
and bear the common name Scanning Proximity Probe Microscopy (SPM).
Detailed description of the operation principles and some examples
measured in the Lab 219, Semiconductor Laboratory, Faculty of Physics, Sofia University,
Galitchica str. 33A, Sofia, in Bulgarian language is here
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Atomic Force Microscopes from Anfatec Instruments (Germany)
Distributed in the Balkan countries by Advanced Technologies Ltd. (Bulgaria)
You get the attention and individual treatment only a small,
family company with traditions (Anfatec was incorporated in 1996) can provide. Within
24 hours you get access directly to the designer and manufacturer of the AFM. Open
software for system control, thus it is easy to implement original experiments.
Big web site for AFM support from Advanced Technologies Ltd. A range of samples
and student exercises with step by step explanations. Infrastructure for distant
education is being developed in the Faculty of Physics, Sofia University, Bulgaria.
Remote access and online support is possible. Help in developing and translating
student exercises and adding novel experiments.
Prices
are in the range 20000-39000 €. Universities in most countries here
are free from VAT for products produced in Europe. At these prices tenders are usually
not compulsory.
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Si (111) steps. 1 x 1 µm scan. |
Main features and characteristics of the Anfatec Level AFM:
- Best
value / price ratio on the market combined with the famous German quality;
- A possibility to visualize features below the surface is being developed using
the idea published in a paper in "Science" in 2005. When implemented there will
be an easy upgrade path;
- Both dynamic (tapping mode) and contact mode of operation;
- Large range of experimental methods: topography (AFM), friction (Friction Force
Microscopy), magnetic forces (Magnetic Force Microscopy), electrical forces (Electrical
Force Microscopy), elasticity of the substrate (Phase contrast imaging), capacity
(Scanning Capacitance Microscopy), surface conductivity (Conductive AFM), work function
(Kelvin Probe Force Microscopy (KPFM)). Anfatec are worldwide leaders in KPFM. Electrochemistry
cell is under development.
- Built-in 3 levels of vibroisolation, which eliminates the need for additional
vibroisolation: simple antivibration table, granite base plate, body hangs on rubber
bands—the most effective vibroisolation according to scientific papers;
- 3 motors for leveling the sample. This greatly increases the number of samples
that can be viewed without additional preparation and represents the newest trend
in AFMs;
- Lateral resolution is limited by the fact that measurements are made in ambient
air. Achievable lateral resolution in air < 5 nm. Technical resolution < 0.2
nm;
- Achievable vertical resolution < 0.1 nm (atomic steps). See the Si (111)
figure above for example;
- One of the fastest control electronics on the market. Data refresh rate—40
kHz, bandwidth of the amplifiers7—over 700 kHz;
- Scan range (typical) on X and Y-48 µm, on Z-8µm. Manual sample positioning
with precision screws—6 mm;
- Hardware (on all 3 axis!) and software linearization of the scanner;
- Possibility to gather data with high resolution: up to 2048 x 2048 points on
all 8 channels;
- Built-in video camera with focusing optics and two levels of illumination;
- Two built-in dual phase low-noise lock-in amplifiers with more than 1 MHz bandwidth;
- Possibility to collect and visualize data on up to 8 channels simultaneously;d
- 15 step by step student exercises with samples to measure;
- The control software is with open license and the source code is freely distributed.
Amendments to the software can be made by the manufacturer upon request. Free upgrade
to newer versions. The possibility to adapt the software to different languages
is currently being implemented.
- Powerful analyzing software is implemented. It has the possibility to do 3D
visualization and rotation of the image, filtering and up to 2D leveling, calculations
(e.g. roughness), picture optimization, etc. Inexpensive additional licenses so
you can make demos on your laptop for example.
- The price includes a number of cantilevers (depending on system ordered);
- Included is a powerful low-noise desktop computer with two 19" LCD monitors;
- Two years of warrant
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A very difficult sample to measure. A monolayer from 30 nm ferrite
spheres covered with oleic acid, deposited on a Si wafer. Measured in dynamic mode
with sharpened tip. Measurement was done in a conference environment without the
vibration isolation table. Individual spheres can clearly be seen. As well as some
tree like aggregation of a bigger size spheres. Same sample in same environment
was measured by a top of the line competitor's instrument costing over 160 000 €
but did not reveal a better picture. See end of page.
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Web site: Anfatec Instruments AG (Germany):www.anfatec.de
Some more images:
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